50L New Type Glass Jacketed Reactor/ Double Layer Glass Reactor with Heating Bath
Circulation liquid of hot, cold or cryogenic can be filled into the jacket of reactor. Substance reacts by stirring under normal or negative pressure in aieproof glass container. Reaction process can be watched clearly through crystal reaction flask. Jacket Glass Reactor is ideal equipment in library experiment or medium-production in moden biology and pharmcy, and is also applied in synthesizing materials in fine chemical industry.
Working principle:
This machine has electric constant speed stirring system, condensation and dropping system. The interlayer of kettle body needs to be connected with heating or cooling circulation equipment. When the material is stirred, the circulating hot solution or cooling liquid is injected through the interlayer to make the materials in the kettle are heated or cooled at a constant temperature. When the material is heated and reacted, the evaporation efficiency can be improved under vacuum conditions (a vacuum device need to be connected). The solvent vapor is cooled into liquid when passing through the glass condensing coil (a cooling device need to be connected), which can be refluxed into the kettle. It can also be recycled through the lower valve of the dean-stark. When the reaction is completed, the material can be discharged from the side outlet at the bottom of the kettle.
This series of products need to be equipped with a vacuum device, a high-temperature or low-temperature circulation device to form system devices.
Basic configuration
• The parts in contact with the material are all made of high borosilicate glass (expansion coefficient 3.3) and PTFE materials, which have stable performance and are not easy to react with the materials.
• Using aluminum alloy + stainless steel material as frame body
• Glass + PTFE discharge valve, side material discharge without effusion.
• Low-speed power-increasing motor, electronic stepless speed regulation, fine adjustment by knob, speed control box with dual display function can digitally display the speed and the temperature of the material in the kettle.
• The stirring system adopts ceramic bearings and mechanical seals to prevent the stirring rod from wearing out.
• Using PT100 temperature sensor, 304 stainless steel material, wrapped by transparent PTFE tube outside , double anti-corrosion.
• Vacuum pressure gauge shows real-time vacuum by pointer.
• Crescent-type stirring paddle, 304 stainless steel + PTFE stirring blade; the material of the stirring rod is 304 stainless steel, and it is wrapped in PTFE tube outside.
• There is a universal wheel with brake at the bottom of the equipment, which can be moved as a whole and be operated conveniently.
• Fuse safety protection
Technical Parameters :
| Model |
HEB-50L |
| Reactor volume |
50L, inner diameter 365mm, outer diameter 410mm, inner length 576mm |
| Interlayer volume |
About 16L |
| Voltage/Frequency |
220V 50HZ/110V 60Hz |
| Stirring motor power |
120W1/3 |
| Stirring speed |
0-450rpm/min |
| Temperature range of reactor |
-80ºC~+250ºC |
| Temperature measuring accuracy |
±1ºC |
| Vacuum |
0.098Mpa |
Kettle lid
Φ265mm
6 ports |
Stirring port |
Φ50mm flange port |
| Condensing reflux port |
50# ball mill port |
| Port of constant pressure funnel |
40# standard port |
| Pressure relief port |
34# standard port |
| Temperature measuring port |
Φ45mm flange port |
| Solid feeding port |
Φ80mm flange port, inner diameter Φ60mm, supporting PTFE cap |
| Stirring paddle |
Φ17×1000H(mm) blade 190mm |
| Condenser |
Φ100mm×700H(mm) lower Φ60mm flange port |
| Condensing area |
0.4 |
| Dean-stark |
Upper Φ60 flange port, left 50# ball mill stopper |
| Constant pressure funnel |
2L, upper 29# standard port with glass stopper; lower 40#standard stopper |
| Pressure relief valve |
34# standard plug valve, releasing valve (pagoda joint) with 12mm outer diameter |
| Inlet and outlet circulation port of interlayer |
Φ45mm flange port supporting flange plate, 1/2" male-PNT adapter |
| Material discharging port |
Φ75mm flange, Φ33mm material discharging hole, oblique discharging valve(pagoda joint)Φ34mm, 350mm from the ground
|
| Vacuum nozzle |
Pagoda joint with 12mm outer diameter |
| In and out circulating nozzle of condenser coil |
Pagoda joint with 15mm outer diameter |
| Overall dimension(W*D*H) |
870×560×2270mm |
| Net weight |
67KG |
| Packing dimension |
1690×615×880mm wooden package 0.92m³ |
| Packing weight |
104KG |
Package & Delivery:
Factory:
Certification:
Trade fair picture:
Customer's feedback:
FAQ:
1. Are you the factory?
Yes, we're.
Established in 2008, we manufacture rotary evaporator, jacketed glass reactor, chiller etc.
2. What is the delivery time?
Generally speaking, the delivery time is 7-10 days for regular products. For the customized instrument, about 10~20 days is needed.
3. What's the warranty period? How do you provide this?
One year (12 months).
We have very strict inspection and testing to make sure the instruments which you received are high-quality and reliable.
If there's any problem, we'll provide you the on line solution in 12 hours. If the problem is caused by accessory, we'll provide you the spare parts for free. If the problem is caused by the instrument quality, and cannot be repaired, we'll ship you the new one.
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