| Customization: | Available |
|---|---|
| After-sales Service: | Yes |
| Warranty: | 1 Year |
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50L Lifting and rotating jacketed glass reactor
Product introduction:
This machine has electric constant speed stirring system, condensation and dropping system. The interlayer of kettle body needs to be connected with heating or cooling circulation equipment. When the material is stirred, the circulating hot solution or cooling liquid is injected through the interlayer to make the materials in the kettle are heated or cooled at a constant temperature. When the material is heated and reacted, the evaporation efficiency can be improved under vacuum conditions (a vacuum device need to be connected). The solvent vapor is cooled into liquid when passing through the glass condensing coil (a cooling device need to be connected), which can be refluxed into the kettle. It can also be recycled through the lower valve of the dean-stark. When the reaction is completed, the material can be discharged from the side outlet at the bottom of the kettle.
The lifting and rotating reactor is based on the ordinary reactor, but it can raise the kettle cover and the upper part of the kettle cover as a whole. After the stirring rod leaves the kettle body, the kettle body can be rotated 150 degrees to the left through the handwheel to pour out the materials directly, which is easy to clean the kettle body.
This series of products need to be equipped with a vacuum device, a high-temperature or low-temperature circulation device to form system devices.
Basic configuration:
• The parts in contact with the material are all made of high borosilicate glass (expansion coefficient 3.3) and PTFE materials, which have stable performance and are not easy to react with the materials.
• The main stent is made of square steel anti-corrosive spray + aluminum alloy + stainless steel.
• Using PTFE material as kettle cover.
• The kettle cover and the upper part of the kettle cover can be lifted and lowered electrically, and the kettle body can be rotated 150° to the left by the handwheel.
• Glass + PTFE discharging valve, side material discharge without effusion.
• Buffer device: connect the inlet and outlet of jacket with stainless steel hoses, fix them to the stent and then connect with the external circulation pipe to reduce the pressure of the inlet and outlet liquids. It can also avoid the damage to the connection part of the glass interlayer circulation port and the circulation pipe .
• Low-speed power-increasing motor, frequency control of motor speed, fine adjustment by knob, speed control box with dual display function can digitally display the speed and the temperature of the material in the kettle.
• The stirring system adopts ceramic bearings and mechanical seal to prevent abrasion of the stirring rod.
• Using PT100 temperature sensor, 304 stainless steel material, wrapped by transparent PTFE tube , double anti-corrosion.
• Vacuum pressure gauge shows real-time vacuum by pointer.
• Crescent-type stirring paddle, 304 stainless steel + PTFE stirring blade; the material of the stirring rod is 304 stainless steel, and it is wrapped in PTFE tube outside.
• The bottom of the machine is equipped with universal wheel with brake, which can be moved as a whole and be operated conveniently.
• Stirring, lifting fuse safety protection.
Technical parameter:
| Model | SJHEB-50L | |
| Reactor volume | 50L, inner diameter 365mm, outer diameter 410mm, inner length 576mm | |
| Interlayer volume | About 16L | |
| Voltage/Frequency | 220V 50Hz/110V 60Hz | |
| Total power | 160W | |
| Stirring motor power | 120W1/3 | |
| Lifting motor power | 40W1/12.5 | |
| Stirring speed | 0-450rpm/min | |
| Temperature range of reactor | -80ºC~ +250ºC | |
| Temperature measuring accuracy | ±1ºC | |
| Vacuum | 0.098Mpa | |
| Kettle cover Φ265mm 6 ports (PTFE cover) |
Stirring port | Φ50mm threaded port |
| Condensing reflux port | 50# ball mill port | |
| Port of constant pressure funnel | 40# standard port | |
| Pressure relief port | 34# standard port | |
| Temperature measuring port | 24# standard port | |
| Socover feeding port | Φ80mm threaded port, inner diameter 50#mm | |
| Stirring paddle | Φ17×1000H(mm) blade 190mm | |
| Condenser | Φ120×600H(mm) lower Φ60 flange port | |
| Condensation area | 0.5m2 | |
| Dean-stark | Upper Φ60 flange port, left 50# ball mill stopper | |
| Constant pressure funnel | 2L, upper 29# standard port with glass stopper; lower 40#standard stopper, lower equipped with 40# standard port×40#standard stopper, s type adapter connected with kettle cover | |
| Pressure relief valve | 34# standard plug valve, releasing valve(pagoda joint) with 12mm outer diameter | |
| Inlet and outlet circulation port of interlayer | Φ45mm flange port supporting 3/4" buffer device, 1/2" adapter as external interface | |
| Material discharging port | Φ75 flange port, Φ33mm material discharging hole, oblique discharging port(pagoda joint)Φ34mm, 290mm from the ground | |
| Vacuum nozzle | Pagoda joint with 12mm outer diameter | |
| In and out circulating nozzle of condenser coil | Pagoda joint with 15mm outer diameter | |
| Lift stroke of reactor | 740mm(The stirring rod shall be 50mm away from the top of the kettle cover) | |
| Kettle rotation | Rotate 150° to the left | |
| Overall dimension(W*D*H) | 750×950×(2320-2950 after lifting)mm | |
| Net weight | 148KG | |
| Packing dimension | 2380×680×1080mm wooden package 1.75m³ | |
| Packing weight | 225KG | |
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